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Alex Ulianytskyi committed 118f6c4

Лаба №12

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File 12/lab-12.tex

+\documentclass[a4paper,10pt]{article}
+\usepackage[left=2cm,right=2cm,top=2cm,bottom=2cm,bindingoffset=0cm]{geometry}
+\usepackage[utf8]{inputenc}
+\usepackage[T2A]{fontenc}
+\usepackage[ukrainian]{babel}
+\usepackage{indentfirst,mathenv,amsmath,array}
+\usepackage[pdftex]{graphicx}
+\graphicspath{{images/}}
+\usepackage[pdftex,unicode,colorlinks]{hyperref}
+\hypersetup{
+    pdftitle={Лабораторна робота №12},
+    pdfauthor={Ульяницький Олександр}
+}
+%opening
+\title{\emph{Лабораторна робота №12}\\Визначення оптичних характеристик люмінесцентних
+індикаторів на прикладі саліцилової кислоти}
+\author{Ульяницький Олександр}
+
+\begin{document}
+\maketitle
+\section*{Мета роботи}
+Перевірити правило дзеркальної симетрії Льовшина на прикладі саліцилової кислоти.
+\section*{Розчини}
+Стандартний розчин саліцилової кислоти (рис. \ref{fig:salicylic_acid})
+\begin{figure}[htp!]
+ \centering
+ \includegraphics[height=2cm]{Salicylic-acid-skeletal.png}
+ % Salicylic-acid-skeletal.png: 256x279 pixel, 72dpi, 9.03x9.84 cm, bb=0 0 256 279
+ \caption{Саліцилова кислота}
+ \label{fig:salicylic_acid}
+\end{figure}
+\section*{Посуд та обладнання}
+\begin{enumerate}
+    \item Кювета скляна з $l=1,0$ см
+    \item Спектрофотометр ``UNICO 2800''
+    \item Спектрофлулориметр ``UNICO LS-55''
+\end{enumerate}
+\section*{Порядок виконання роботи}
+\begin{enumerate}
+\item Вимірюють спектр поглинання р-ну саліцилової кислоти з концентрацією $10^{-5}$ моль/л в діапазоні 190--400 нм (рис. \ref{fig:absorption}) при pH = 5,2, $\lambda_\mathrm{max}=298$ нм.
+\begin{figure}[htp!]
+ \centering
+ \includegraphics{apsorption_spectrum.pdf}
+ \caption{Спектр поглинання саліцилової кислоти. $C=10^{-5}$ моль/л, pH = 5,2, $l=1,0$ см.}
+ \label{fig:absorption}
+\end{figure}
+
+\item Вимірюють спектр збудження для р-ну саліцилової кислоти з концентрацією $10^{-6}$ моль/л в діапазоні 200--800 нм (рис. \ref{fig:emission}) при pH = 5,2. Знаходять довжину хвилі при максимумі збудження --- $\lambda_\textrm{збудж.}=300$ нм.
+\begin{figure}[htp!]
+ \centering
+ \includegraphics{emission_spectrum.pdf}
+ \caption{Спектр збудження саліцилової кислоти. $C=10^{-6}$ моль/л, pH = 5,2, $l=1,0$ см}
+ \label{fig:emission}
+\end{figure}
+
+\item Вимірюють спектр флуорисценції р-ну саліцилової кислоти з концентрацією $10^{-6}$ моль/л при pH = 5,2 та $\lambda_\textrm{збудж.}=300$ нм. (рис. \ref{fig:luminescence})
+\begin{figure}[htp!]
+ \centering
+ \includegraphics{luminescence_spectrum.pdf}
+ \caption{Спектр люмінесценції саліцилової кислоти при $\lambda_\textrm{збудж.}=300$ нм. $C=10^{-6}$ моль/л, pH = 5,2, $l=1,0$ см}
+ \label{fig:luminescence}
+\end{figure}
+
+\item Також наведений спектр збудження при $\lambda_\textrm{люмін.}=412$ нм (рис. \ref{fig:emission_412}).
+\begin{figure}[htp!]
+ \centering
+ \includegraphics{emission_412_spectrum.pdf}
+ \caption{Спектр збудження саліцилової кислоти при $\lambda_\textrm{люмін.}=412$ нм. $C=10^{-6}$ моль/л, pH = 5,2, $l=1,0$ см}
+ \label{fig:emission_412}
+\end{figure}
+
+\item Нормують спектри у координатах $I/I_\mathrm{max} = f(\nu),~\textrm{см}^{-1}$ для флуорисценції
+та у координатах $\varepsilon/\varepsilon_\mathrm{max} = f(\nu),~\textrm{см}^{-1}$ (рис. \ref{fig:normal}). Знаходять точку перетину спектрів --- $\nu_0$.
+\begin{figure}[htp!]
+ \centering
+ \includegraphics{norm_spectra.pdf}
+ % norm_spectra.pdf: 465x226 pixel, 72dpi, 16.40x7.97 cm, bb=0 0 465 226
+ \caption{Нормовані спектри поглинання та флуорисценйії саліцилової кислоти.}
+ \label{fig:normal}
+\end{figure}
+
+\item \paragraph*{Перевірка правила Льовшина.} Значення $(\nu^\mathrm{max}_{abs} + \nu^\mathrm{max}_{fl})/\nu_0$ повинно бути приблизно рівне 2. Значення для саліцилової кислоти \eqref{eq:lv-sal}:
+\begin{equation}
+ \label{eq:lv-sal}
+ \frac{\nu^\mathrm{max}_{abs} + \nu^\mathrm{max}_{fl}}{\nu_0} = \frac{43478,3 + 24301,3}{30581,0} = 2,21639 \approx 2
+\end{equation}
+\end{enumerate}
+
+\section*{Висновки}
+На лабораторній роботі було експериментально підтверджено правило дзеркальної симетрії Льовшина на прикладі саліцилової кислоти.
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